Biopolymer-assisted green synthesis of functional cerium oxide nanoparticles
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Tarih
2020
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Springer International Publishing Ag
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
Cerium oxide nanoparticles were synthesized by thermal decomposition of cerium alginate biopolymer gel at 450 degrees C, where alginate both acts as a precursor and a template. The synthesis is a green, facile and one-step method and the resulting nanoparticles have functionalized surface. The resulted material were characterized using X-ray diffraction for confirmation of cerium oxide, crystallite size analysis and grain size distribution. Transmission electron microscopy was used for the particle size determination, hydrodynamic size estimation was studied by dynamic light scattering and surface characteristics were analyzed using zeta potential measurements. Results show the presence of spherical particles with a size of < 5 nm. Having only a negative surface charge in such a wide pH range will ensure that the behavior of obtained nanoparticles in different environments is predictable. Isoelectric point of the synthesized material is significantly different from non-functionalized cerium oxide, and indicates the surface functionality, which is an important property for biocompatibility.
Açıklama
Erim, Fatma Bedia/0000-0001-9406-6681
Anahtar Kelimeler
Cerium Oxide, Functional, Nanoparticle, Alginate, Thermal Decomposition
Kaynak
Chemical Papers
WoS Q Değeri
Q3
Scopus Q Değeri
Q2
Cilt
74
Sayı
7